Kivrak, HilalKhalid, SarwarCaglar, AykutAlpaslan, DuyguSelcuk, KadirDudu, Tuba ErsenAktas, Nahit2025-05-102025-05-1020222578-486210.1002/est2.2862-s2.0-85159775692https://doi.org/10.1002/est2.286https://hdl.handle.net/20.500.14720/8501Kivrak, Hilal/0000-0001-8001-7854; Alpaslan, Duygu/0000-0002-6007-3397At present, poly(methacrylic acid) (MA), poly(MA) hydrogel, and Pd-doped poly(MA) hydrogel modified electrodes are constructed on graphite pencil (G). The Pd precursor is coated on the poly(MA)/G electrodes surface using the electrodeposition method. These electrodes are characterized by thermogravimetric analysis (TGA), Fourier transform infrared spectroscopy, and scanning electron microscopy-energy dispersive X-ray. Poly(MA) hydrogel and Pd-doped poly(MA) hydrogel are successfully prepared by the polymerization and further electrodeposition. Formic acid electro-oxidation (FAEO) activities are examined with cyclic voltammetry (CV), chronoamperometry (CA), and electrochemical impedance spectroscopy (EIS). Poly(MA)/G and Pd doped poly(MA) electrodes exhibit promising electro-catalytic activity with 60 mA current density, greater than literature values. Pd-doped poly(MA) hydrogel electrodes are promising electrodes for FAEO.eninfo:eu-repo/semantics/closedAccessElectrodepositionElectro-OxidationFormic AcidPdPoly(Methacrylic Acid)Article41N/AQ3WOS:000705178000001