Aslanoglu, Furgan2025-05-102025-05-1020220022-152X1943-519310.1002/jhet.44822-s2.0-85127340314https://doi.org/10.1002/jhet.4482https://hdl.handle.net/20.500.14720/14135Aslanoglu, Furgan/0000-0002-5740-1716An interesting synthesis method for 2-acetate-1-(2-pyrrolidinone)-butane-1,3-dione compounds was developed in this work. The synthesis of these compounds was carried out in three steps. In the first step, 2-pyrrolidone derivatives were obtained by the Friedel-Crafts reaction in presence of Eaton's reagent. Then, -NH group of 2-pyrrolidone compounds were attached acetoacetate group in presence of 2,6-trimethyl-4H-1,3-dioxin-4-one reagent. Lastly, 1-(2-pyrrolidinone)-butane-1,3-dione derivatives were reacted with Pida to attach acetoxy group to these compound's methylene.eninfo:eu-repo/semantics/closedAccessDesign of 1-(2 Derivatives and Acetoxylation of These Compound's Methylene Via Hypervalent Iodine (Iii)Article599Q2Q216601663WOS:000776345800001