Developing a New and Simple Ultrasound-Assisted Emulsification Liquid Phase Microextraction Method Built Upon Deep Eutectic Solvents for Patent Blue V in Syrup and Water Samples
dc.authorid | Soylak, Mustafa/0000-0002-1017-0244 | |
dc.authorid | Yilmaz, Erkan/0000-0001-8962-3199 | |
dc.authorscopusid | 56841645900 | |
dc.authorscopusid | 55415378600 | |
dc.authorscopusid | 7006488616 | |
dc.authorwosid | Soylak, Mustafa/K-7956-2012 | |
dc.authorwosid | Yilmaz, Erkan/Aab-6178-2020 | |
dc.contributor.author | Kanberoglu, Gulsah Saydan | |
dc.contributor.author | Yilmaz, Erkan | |
dc.contributor.author | Soylak, Mustafa | |
dc.date.accessioned | 2025-05-10T17:33:54Z | |
dc.date.available | 2025-05-10T17:33:54Z | |
dc.date.issued | 2019 | |
dc.department | T.C. Van Yüzüncü Yıl Üniversitesi | en_US |
dc.department-temp | [Kanberoglu, Gulsah Saydan] Van YuzuncuYil Univ, Fac Sci, Dept Chem, TR-65080 Van, Turkey; [Yilmaz, Erkan] Erciyes Univ, Fac Pharm, Dept Analyt Chem, TR-38039 Kayseri, Turkey; [Yilmaz, Erkan] Erciyes Univ, Nanotechnol Res Ctr ERNAM, TR-38039 Kayseri, Turkey; [Soylak, Mustafa] Erciyes Univ, Fac Sci, Dept Chem, TR-38039 Kayseri, Turkey | en_US |
dc.description | Soylak, Mustafa/0000-0002-1017-0244; Yilmaz, Erkan/0000-0001-8962-3199 | en_US |
dc.description.abstract | In this study, Deep Eutectic Solvents (DESs) were utilized for ultrasound -assisted emulsification liquid phase microextraction (UA-ELPME) of Patent Blue V in syrup and water samples. Patent Blue V in sample solution of pH 4.0 was extracted into DES phase prepared from choline chloride and phenol. Concentration of Patent Blue V in final DES phase was measured at 627.5 nm with Uv-Vis spectrophotometry. Sample volume, pH, matrix effect, volume and type of DES, ultrasonication and centrifugation times were investigated and optimized. The developed UA-ELPME method presents a limit of detection (LOD) of 0.37 mu g L-1, preconcentration factor of 15 and a relative standard deviation (RSD, %) of 6.0% under the optimum conditions. The validation was carried out with standard addition-recovery experiments for syrup and water samples. The obtained recovery results showed that the developed UA-ELPME method was applicable for routine Patent Blue V analysis in syrup and water samples. | en_US |
dc.description.woscitationindex | Science Citation Index Expanded | |
dc.identifier.doi | 10.1016/j.microc.2018.11.053 | |
dc.identifier.endpage | 818 | en_US |
dc.identifier.issn | 0026-265X | |
dc.identifier.issn | 1095-9149 | |
dc.identifier.scopus | 2-s2.0-85057821332 | |
dc.identifier.scopusquality | Q1 | |
dc.identifier.startpage | 813 | en_US |
dc.identifier.uri | https://doi.org/10.1016/j.microc.2018.11.053 | |
dc.identifier.uri | https://hdl.handle.net/20.500.14720/13615 | |
dc.identifier.volume | 145 | en_US |
dc.identifier.wos | WOS:000457513000105 | |
dc.identifier.wosquality | Q1 | |
dc.language.iso | en | en_US |
dc.publisher | Elsevier Science Bv | en_US |
dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |
dc.rights | info:eu-repo/semantics/closedAccess | en_US |
dc.subject | Deep Eutectic Solvent | en_US |
dc.subject | Ultrasound-Assisted Emulsification Liquid Phase Microextraction | en_US |
dc.subject | Patent Blue V | en_US |
dc.subject | Preconcentration | en_US |
dc.subject | Determination | en_US |
dc.subject | Uv-Vis Spectrophotometry | en_US |
dc.title | Developing a New and Simple Ultrasound-Assisted Emulsification Liquid Phase Microextraction Method Built Upon Deep Eutectic Solvents for Patent Blue V in Syrup and Water Samples | en_US |
dc.type | Article | en_US |