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Developing a New and Simple Ultrasound-Assisted Emulsification Liquid Phase Microextraction Method Built Upon Deep Eutectic Solvents for Patent Blue V in Syrup and Water Samples

dc.authorid Soylak, Mustafa/0000-0002-1017-0244
dc.authorid Yilmaz, Erkan/0000-0001-8962-3199
dc.authorscopusid 56841645900
dc.authorscopusid 55415378600
dc.authorscopusid 7006488616
dc.authorwosid Soylak, Mustafa/K-7956-2012
dc.authorwosid Yilmaz, Erkan/Aab-6178-2020
dc.contributor.author Kanberoglu, Gulsah Saydan
dc.contributor.author Yilmaz, Erkan
dc.contributor.author Soylak, Mustafa
dc.date.accessioned 2025-05-10T17:33:54Z
dc.date.available 2025-05-10T17:33:54Z
dc.date.issued 2019
dc.department T.C. Van Yüzüncü Yıl Üniversitesi en_US
dc.department-temp [Kanberoglu, Gulsah Saydan] Van YuzuncuYil Univ, Fac Sci, Dept Chem, TR-65080 Van, Turkey; [Yilmaz, Erkan] Erciyes Univ, Fac Pharm, Dept Analyt Chem, TR-38039 Kayseri, Turkey; [Yilmaz, Erkan] Erciyes Univ, Nanotechnol Res Ctr ERNAM, TR-38039 Kayseri, Turkey; [Soylak, Mustafa] Erciyes Univ, Fac Sci, Dept Chem, TR-38039 Kayseri, Turkey en_US
dc.description Soylak, Mustafa/0000-0002-1017-0244; Yilmaz, Erkan/0000-0001-8962-3199 en_US
dc.description.abstract In this study, Deep Eutectic Solvents (DESs) were utilized for ultrasound -assisted emulsification liquid phase microextraction (UA-ELPME) of Patent Blue V in syrup and water samples. Patent Blue V in sample solution of pH 4.0 was extracted into DES phase prepared from choline chloride and phenol. Concentration of Patent Blue V in final DES phase was measured at 627.5 nm with Uv-Vis spectrophotometry. Sample volume, pH, matrix effect, volume and type of DES, ultrasonication and centrifugation times were investigated and optimized. The developed UA-ELPME method presents a limit of detection (LOD) of 0.37 mu g L-1, preconcentration factor of 15 and a relative standard deviation (RSD, %) of 6.0% under the optimum conditions. The validation was carried out with standard addition-recovery experiments for syrup and water samples. The obtained recovery results showed that the developed UA-ELPME method was applicable for routine Patent Blue V analysis in syrup and water samples. en_US
dc.description.woscitationindex Science Citation Index Expanded
dc.identifier.doi 10.1016/j.microc.2018.11.053
dc.identifier.endpage 818 en_US
dc.identifier.issn 0026-265X
dc.identifier.issn 1095-9149
dc.identifier.scopus 2-s2.0-85057821332
dc.identifier.scopusquality Q1
dc.identifier.startpage 813 en_US
dc.identifier.uri https://doi.org/10.1016/j.microc.2018.11.053
dc.identifier.uri https://hdl.handle.net/20.500.14720/13615
dc.identifier.volume 145 en_US
dc.identifier.wos WOS:000457513000105
dc.identifier.wosquality Q1
dc.language.iso en en_US
dc.publisher Elsevier Science Bv en_US
dc.relation.publicationcategory Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı en_US
dc.rights info:eu-repo/semantics/closedAccess en_US
dc.subject Deep Eutectic Solvent en_US
dc.subject Ultrasound-Assisted Emulsification Liquid Phase Microextraction en_US
dc.subject Patent Blue V en_US
dc.subject Preconcentration en_US
dc.subject Determination en_US
dc.subject Uv-Vis Spectrophotometry en_US
dc.title Developing a New and Simple Ultrasound-Assisted Emulsification Liquid Phase Microextraction Method Built Upon Deep Eutectic Solvents for Patent Blue V in Syrup and Water Samples en_US
dc.type Article en_US

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