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Electrochemical Determination of Fluoroquinolone Antibiotic Norfloxacin in the Presence of Anionic Surfactant Using the Anodically Pretreated Boron-Doped Diamond Electrode

dc.authorid Senturk, Zuhre/0000-0002-0356-9345
dc.authorid Yardim, Yavuz/0000-0002-9587-096X
dc.authorscopusid 57201902339
dc.authorscopusid 55925456300
dc.authorscopusid 35740840400
dc.authorscopusid 55807475500
dc.authorscopusid 55511747958
dc.authorscopusid 7004177719
dc.authorwosid Talay Pınar, Pınar/Jfj-2292-2023
dc.authorwosid Senturk, Zuhre/Aas-5179-2020
dc.authorwosid Keskin, Ertuğrul/Ael-9615-2022
dc.contributor.author Karahan, Fatih
dc.contributor.author Basi, Zehra
dc.contributor.author Keskin, Ertugrul
dc.contributor.author Pinar, Pinar Talay
dc.contributor.author Yardim, Yavuz
dc.contributor.author Senturk, Zuhre
dc.date.accessioned 2025-05-10T17:07:41Z
dc.date.available 2025-05-10T17:07:41Z
dc.date.issued 2020
dc.department T.C. Van Yüzüncü Yıl Üniversitesi en_US
dc.department-temp [Karahan, Fatih] Van Yuzuncu Yil Univ, Fac Sci, Dept Biochem, TR-65080 Van, Turkey; [Basi, Zehra] Van Yuzuncu Yil Univ, Van Sch Hlth, TR-65080 Van, Turkey; [Keskin, Ertugrul] Adiyaman Univ, Fac Pharm, Dept Analyt Chem, TR-02040 Adiyaman, Turkey; [Pinar, Pinar Talay; Yardim, Yavuz] Van Yuzuncu Yil Univ, Fac Pharm, Dept Analyt Chem, TR-65080 Van, Turkey; [Senturk, Zuhre] Van Yuzuncu Yil Univ, Fac Sci, Dept Analyt Chem, TR-65080 Van, Turkey en_US
dc.description Senturk, Zuhre/0000-0002-0356-9345; Yardim, Yavuz/0000-0002-9587-096X en_US
dc.description.abstract In this article, a simple, fast and inexpensive methodology has been developed for the determination of fluoroquinolone class antibiotic norfloxacin (NFX) in anionic surfactant media (sodium dodecyl sulphate, SDS) using an anodically pretreated boron-doped diamond (APT-BDD) electrode. Cyclic voltammetric studies showed that the NFX gave an irreversible and adsorption controlled anodic oxidation signal at a potential of about +1.32 V on the APT-BDD electrode. The effects of parameters such as the electrode pre-treatment procedure, SDS concentration, and instrumental variables on the electrochemical sensitivity of NFX were evaluated. Under optimized conditions, the linearity was achieved in the range of 0.05 to 4.0 mu g mL(-1) (1.57x10(-7)-1.25x10(-5) mol L-1), with a detection limit of 0.013 mu g mL(-1) (4.07x10(-8) mol L-1) by using square-wave adsorptive stripping voltammetry (SW-AdSV). The feasibility of the developed approach for the quantification of NFX in urine samples was tested. en_US
dc.description.woscitationindex Science Citation Index Expanded
dc.identifier.doi 10.1002/slct.202002921
dc.identifier.endpage 12868 en_US
dc.identifier.issn 2365-6549
dc.identifier.issue 42 en_US
dc.identifier.scopus 2-s2.0-85096010449
dc.identifier.scopusquality Q3
dc.identifier.startpage 12862 en_US
dc.identifier.uri https://doi.org/10.1002/slct.202002921
dc.identifier.uri https://hdl.handle.net/20.500.14720/6843
dc.identifier.volume 5 en_US
dc.identifier.wos WOS:000591276200003
dc.identifier.wosquality Q3
dc.language.iso en en_US
dc.publisher Wiley-v C H verlag Gmbh en_US
dc.relation.publicationcategory Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı en_US
dc.rights info:eu-repo/semantics/closedAccess en_US
dc.subject Norfloxacin en_US
dc.subject Voltammetry en_US
dc.subject Boron-Doped Diamond Electrode en_US
dc.subject Surfactants en_US
dc.subject Urine Samples en_US
dc.title Electrochemical Determination of Fluoroquinolone Antibiotic Norfloxacin in the Presence of Anionic Surfactant Using the Anodically Pretreated Boron-Doped Diamond Electrode en_US
dc.type Article en_US

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