Electrochemical Determination of Fluoroquinolone Antibiotic Norfloxacin in the Presence of Anionic Surfactant Using the Anodically Pretreated Boron-Doped Diamond Electrode
dc.authorid | Senturk, Zuhre/0000-0002-0356-9345 | |
dc.authorid | Yardim, Yavuz/0000-0002-9587-096X | |
dc.authorscopusid | 57201902339 | |
dc.authorscopusid | 55925456300 | |
dc.authorscopusid | 35740840400 | |
dc.authorscopusid | 55807475500 | |
dc.authorscopusid | 55511747958 | |
dc.authorscopusid | 7004177719 | |
dc.authorwosid | Talay Pınar, Pınar/Jfj-2292-2023 | |
dc.authorwosid | Senturk, Zuhre/Aas-5179-2020 | |
dc.authorwosid | Keskin, Ertuğrul/Ael-9615-2022 | |
dc.contributor.author | Karahan, Fatih | |
dc.contributor.author | Basi, Zehra | |
dc.contributor.author | Keskin, Ertugrul | |
dc.contributor.author | Pinar, Pinar Talay | |
dc.contributor.author | Yardim, Yavuz | |
dc.contributor.author | Senturk, Zuhre | |
dc.date.accessioned | 2025-05-10T17:07:41Z | |
dc.date.available | 2025-05-10T17:07:41Z | |
dc.date.issued | 2020 | |
dc.department | T.C. Van Yüzüncü Yıl Üniversitesi | en_US |
dc.department-temp | [Karahan, Fatih] Van Yuzuncu Yil Univ, Fac Sci, Dept Biochem, TR-65080 Van, Turkey; [Basi, Zehra] Van Yuzuncu Yil Univ, Van Sch Hlth, TR-65080 Van, Turkey; [Keskin, Ertugrul] Adiyaman Univ, Fac Pharm, Dept Analyt Chem, TR-02040 Adiyaman, Turkey; [Pinar, Pinar Talay; Yardim, Yavuz] Van Yuzuncu Yil Univ, Fac Pharm, Dept Analyt Chem, TR-65080 Van, Turkey; [Senturk, Zuhre] Van Yuzuncu Yil Univ, Fac Sci, Dept Analyt Chem, TR-65080 Van, Turkey | en_US |
dc.description | Senturk, Zuhre/0000-0002-0356-9345; Yardim, Yavuz/0000-0002-9587-096X | en_US |
dc.description.abstract | In this article, a simple, fast and inexpensive methodology has been developed for the determination of fluoroquinolone class antibiotic norfloxacin (NFX) in anionic surfactant media (sodium dodecyl sulphate, SDS) using an anodically pretreated boron-doped diamond (APT-BDD) electrode. Cyclic voltammetric studies showed that the NFX gave an irreversible and adsorption controlled anodic oxidation signal at a potential of about +1.32 V on the APT-BDD electrode. The effects of parameters such as the electrode pre-treatment procedure, SDS concentration, and instrumental variables on the electrochemical sensitivity of NFX were evaluated. Under optimized conditions, the linearity was achieved in the range of 0.05 to 4.0 mu g mL(-1) (1.57x10(-7)-1.25x10(-5) mol L-1), with a detection limit of 0.013 mu g mL(-1) (4.07x10(-8) mol L-1) by using square-wave adsorptive stripping voltammetry (SW-AdSV). The feasibility of the developed approach for the quantification of NFX in urine samples was tested. | en_US |
dc.description.woscitationindex | Science Citation Index Expanded | |
dc.identifier.doi | 10.1002/slct.202002921 | |
dc.identifier.endpage | 12868 | en_US |
dc.identifier.issn | 2365-6549 | |
dc.identifier.issue | 42 | en_US |
dc.identifier.scopus | 2-s2.0-85096010449 | |
dc.identifier.scopusquality | Q3 | |
dc.identifier.startpage | 12862 | en_US |
dc.identifier.uri | https://doi.org/10.1002/slct.202002921 | |
dc.identifier.uri | https://hdl.handle.net/20.500.14720/6843 | |
dc.identifier.volume | 5 | en_US |
dc.identifier.wos | WOS:000591276200003 | |
dc.identifier.wosquality | Q3 | |
dc.language.iso | en | en_US |
dc.publisher | Wiley-v C H verlag Gmbh | en_US |
dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |
dc.rights | info:eu-repo/semantics/closedAccess | en_US |
dc.subject | Norfloxacin | en_US |
dc.subject | Voltammetry | en_US |
dc.subject | Boron-Doped Diamond Electrode | en_US |
dc.subject | Surfactants | en_US |
dc.subject | Urine Samples | en_US |
dc.title | Electrochemical Determination of Fluoroquinolone Antibiotic Norfloxacin in the Presence of Anionic Surfactant Using the Anodically Pretreated Boron-Doped Diamond Electrode | en_US |
dc.type | Article | en_US |