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Facile and Rapid Synthesis of Microwave Assisted Pd Nanoparticles as Non-Enzymatic Hydrogen Peroxide Sensor

dc.authorid Kivrak, Hilal/0000-0001-8001-7854
dc.authorid Kivrak, Arif/0000-0003-4770-2686
dc.authorscopusid 58324442300
dc.authorscopusid 25959155500
dc.authorscopusid 8694518300
dc.authorscopusid 57189211902
dc.authorscopusid 56728563800
dc.authorscopusid 56728709700
dc.authorwosid Kivrak, Arif/Aaq-8432-2021
dc.authorwosid Kivrak, Hilal/Hji-7095-2023
dc.authorwosid Kivrak, Hilal/Aaq-8663-2021
dc.authorwosid Kivrak, Arif/W-2196-2017
dc.contributor.author Sahin, Ozlem
dc.contributor.author Kivrak, Hilal
dc.contributor.author Kivrak, Arif
dc.contributor.author Kazici, Hilal Celik
dc.contributor.author Alal, Orhan
dc.contributor.author Atbas, Dilan
dc.date.accessioned 2025-05-10T17:28:40Z
dc.date.available 2025-05-10T17:28:40Z
dc.date.issued 2017
dc.department T.C. Van Yüzüncü Yıl Üniversitesi en_US
dc.department-temp [Sahin, Ozlem] Selcuk Univ, Dept Chem Engn, Konya 42031, Turkey; [Kivrak, Hilal; Kazici, Hilal Celik; Alal, Orhan; Atbas, Dilan] Yuzuncu Yil Univ, Dept Chem Engn, Van 65081, Turkey; [Kivrak, Arif] Yuzuncu Yil Univ, Dept Chem, Van 65081, Turkey en_US
dc.description Kivrak, Hilal/0000-0001-8001-7854; Kivrak, Arif/0000-0003-4770-2686 en_US
dc.description.abstract Carbon supported Pd catalyst was prepared with microwave-assisted polyol method (M-Pd@C) and investigated sensing activity for non-enzymatic hydrogen peroxide (H2O2). Moreover, M-Pd@C and Pd@C catalyst which synthesized via polyol method (P-Pd@C) were compared to each other in terms of electrocatalytic activity. X-ray diffraction (XRD), X-ray photo electron spectroscopy (XPS), scanning electron microscopy (SEM) and transmission electron microscopy (TEM) were used to investigate structural and morphological properties of these catalysts. Furthermore, electrochemical measurements were performed via cyclic voltammetry (CV), chronoamperometry (CA) techniques. CV results exhibited that M-Pd/C catalyst showed perfect electrocatalytic activity in terms of reduction of H2O2. M-Pd/C catalyst showed a fast response of less than 7 s with a linear range of 5.0x10(-3)-11.0 mM and a relatively low detection limit of 1.2 mu M amperometric response. M-Pd/C catalyst exhibited great selectivity for detecting H2O2 in the existence of several hindering species such as uric acid and ascorbic acid. en_US
dc.description.sponsorship Scientific and Technological Research Council of Turkey (TUBITAK) project [113Z249, 114M156, 114Z042] en_US
dc.description.sponsorship CHI 660E potentiostat employed in electrochemical measurements was purchased from The Scientific and Technological Research Council of Turkey (TUBITAK) project (project no: 113Z249). The chemicals were purchased from TUBITAK project (Project no: 114M156). Anton Paar monowave reactor was purchased from TUBITAK project (project no: 114Z042). XRD measurements were performed at Selcuk University central laboratory. XPS and TEM measurements were conducted at METU central laboratory. en_US
dc.description.woscitationindex Science Citation Index Expanded
dc.identifier.doi 10.20964/2017.01.26
dc.identifier.endpage 769 en_US
dc.identifier.issn 1452-3981
dc.identifier.issue 1 en_US
dc.identifier.scopus 2-s2.0-85009923601
dc.identifier.scopusquality Q3
dc.identifier.startpage 762 en_US
dc.identifier.uri https://doi.org/10.20964/2017.01.26
dc.identifier.uri https://hdl.handle.net/20.500.14720/12109
dc.identifier.volume 12 en_US
dc.identifier.wos WOS:000396470000064
dc.identifier.wosquality Q4
dc.language.iso en en_US
dc.publisher Esg en_US
dc.relation.publicationcategory Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı en_US
dc.rights info:eu-repo/semantics/openAccess en_US
dc.subject Pd Nanoparticles en_US
dc.subject Microwave Assisted Polyol Method en_US
dc.subject Non-Enzymatic en_US
dc.subject Hydrogen Peroxide Sensor en_US
dc.title Facile and Rapid Synthesis of Microwave Assisted Pd Nanoparticles as Non-Enzymatic Hydrogen Peroxide Sensor en_US
dc.type Article en_US

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