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Intermolecular Heterocyclization of Alkynones With 2-Mercaptoacetaldehyde Under Metal-Free Conditions: Synthesis of 2,3-Disubstituted Thiophenes

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Date

2015

Journal Title

Journal ISSN

Volume Title

Publisher

Pergamon-elsevier Science Ltd

Abstract

A concise and regioselective approach for the synthesis of 2,3-disubstituted thiophene derivatives has been developed. The synthetic strategy relies on the reaction of an in situ generated 2-mercaptoacetaldehyde with various alkynones. Furthermore, we calculated the energy gap between the HOMO and the LUMO orbitals of all compounds and observed that the introduction of a strong electron-withdrawing group decreased the HOMO-LUMO energy gap. (C) 2015 Elsevier Ltd. All rights reserved.

Description

Menges, Nurettin/0000-0002-5990-6275

Keywords

Alkynes, Cyclization, Alkynones, 2-Mercaptoacetaldehyde, 2,3-Disubstituted Thiophenes

Turkish CoHE Thesis Center URL

WoS Q

Q3

Scopus Q

Q3

Source

Volume

56

Issue

40

Start Page

5386

End Page

5389